Course Content
Matter
OBJECTIVES By the end of this topic, the trainee should be able to 1.Define matter 2.Explain state of matter 3.Distinguish between physical and chemical changes 4.Explain the gas laws
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Atoms , Elements and Compounds
OBJECTIVES By the end of this topic , the trainee should be able to; 1.Define Elements, Compounds and Mixtures 2.Describe the structure of an atom 3.Describe how to determine the Atomic number ,Mass number and Isotopes
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The Periodic Table
OBECTIVES By the end of this topic, the trainee should be able to : 1.State the historical contribution on development of the periodic table 2.Explain the periodic trends of elements and their compounds 3.State the diagonal relationships of the periodic table
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The S-Block Element
OBJECTIVES By the end of this topic, the trainee should be able to: 1.Explain the chemistry of group I and II elements 2.State the application of group I and two elements and their compounds
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Chemical Bonds
OBJECTIVES By the end of these topic, the trainee should be able to 1.Identify different types of bonds 2.Describe their properties
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Chemical Equilibrium
OBJECTIVES By the end of this topic , the trainee should be able to : 1.Define chemical equilibria 2.Explain types of equilibria 3.Determine equilibrium constant 4.Describe factors affecting chemical equilibrium
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Introduction To Organic Chemistry
By the end of this topic , the trainee should be able to : 1.Explain the aspects of organic chemistry 2.Describe hydrocarbons 3.Classify organic molecules explain chemical reactions of simple organic molecules 4.Explain the properties , synthesis and uses of simple organic molecules
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Acids, Bases and Salts
OBJECTIVES By the end of this session , the trainee should be able to : 1.State properties of acids and bases 2.Differentiate between strong and weak acids 3.Explain types and properties of salts
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PH Analysis
OBJECTIVES By the end of this topic, the trainee should be able to: 1.Define the term PH 2.Explain the basic theory of PH 3.State the relationship between PH and color change in indicators 4.Explain the term buffer solution 5.Describe the preparation of buffer solutions 6.State the application of buffer solutions
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Sampling and Sample Preparation
OBJECTIVE By the end of this topic, the trainee should be able to : 1.Define the terms used in sample preparation 2.State the importance of sampling 3.Describe the techniques of sampling 4.Describe the procedure for sample pre-treatment 5.State sample storage methods
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Separation Techniques
OBJECTIVES By the end of this topic , the trainee should be able to : 1.Define separation, extraction and purification 2.Describe the separation , extraction and purification techniques 3.Explain the methods of determining purity of substances
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Heating and Cooling Techniques
OBJECTIVES To identify various techniques used for heating and cooling substances in the laboratory
Heating and Cooling Techniques
OBJECTIVES To identify various techniques used for heating and cooling substances in the laboratory
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Distillation Techniques
By end of this topic, Trainee should be able to : 1. Define distilation 2. State and explain various distillation techniques 3. Outline Various distillation techniques 4. Outline the applications of Distillation techniques
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Crystallization Techniques
OBJECTIVES By the end of the topic, the learner should be able to: 1.To define crystallization 2.To describe crystallization process 3.To carry out crystallization procedure
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Solvent Extraction Techniques
OBJECTIVES By the end of the topic, the learner should be able to 1.Define solvent extraction 2.Explain terms used in solvent extraction 3.Describe methods of solvent extraction 4.Describe selection of appropriate solvents for solvent extraction 5.Determine distribution ration 6.Outline factors actors influencing the extraction efficiency 7.Describe Soxhlet extraction
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Chromatography Techniques
OBJECTIVES By the end of this topic, the learner should be able to: 1.Define chromatography techniques 2.Explain terms used in chromatography techniques 3.Describe principles of chromatography techniques 4.Explain types of chromatography techniques 5.Carry out chromatography experiments 6.Determine RF factor 7.Outline electrophoresis
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Titrimetric Analysis
OBJECTIVES By the end of this topic, the trainee should be able to: 1.Define terms used in titrimetric analysis 2.Describe types of titrimetric analysis 3.Balance chemical reactions 4.Work out calculations involved in titrimetric analysis
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Redox Titration
Redox Titration is a laboratory method of determining the concentration of a given analyte by causing a redox reaction between the titrant and the analyte. Redox titration is based on an oxidation-reduction reaction between the titrant and the analyte. It is one of the most common laboratory methods used to identify the concentration of unknown analytes. Redox reactions involve both oxidation and reduction. The key features of reduction and oxidation are discussed below.
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Complexiometric Titration
omplexometric Titration or chelatometry is a type of volumetric analysis wherein the colored complex is used to determine the endpoint of the titration. The method is particularly useful for determination of the exact number of a mixture of different metal ions, especially calcium and magnesium ions present in water in solution .
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Gravimetric Analysis
OBJECTIVES By the end of this topic, the trainee should be able to: 1.Define gravimetric analysis 2.Describe the principles of gravimetric analysis 3.Describe the steps involved in gravimetric analysis 4.Explain factors affecting gravimetric analysis 5.Describe the equipments and apparatus used in gravimetric analysis 6.Carry out gravimetric analysis
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Calorimetric Analysis
OBJECTIVES By the end of this topic, the trainee should be able to: 1.Define terms and units used in thermochemistry 2.Determine enthalpy changes in chemical reactions 3.Determine heat capacity and specific heat capacity 4.Compare calorific values of different materials 5.Determine different heat reactions 6.Apply law of conservation of energy and Hess law in thermochemical calculations
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Chemistry Techniques for Science Laboratory Technicians
About Lesson

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The Periodic Trends

The elements on the periodic table are arranged periodically so that trends can be easily recognized.  Trends run horizontally across the periodic table starting from the left hand-side to the right. For instance , from the period you can easily determine the  following trends

  1. Trends of ionsg. group 1 elements have a +1 ionic charge whereas group two, three, four , five , six and seven have +2,+3,±4,-3,-2,-1 ionic charge respectively
  2. Trends of electronegativity

Another important periodic trend to be aware of is how electronegativity differences can be identified. Electronegativity is the measure of an atom’s tendency to attract a bonding pair of electrons. There are various numerical scales for rating electronegativity. The trends for electronegativity in the periodic table are that electronegativity increases as you go across a period, and increases as you go up a group, with fluorine being the most electronegative atom. Noble gases are given an electronegativity rating of 0 due to their inherent stability, which keeps them from forming bonds with other atoms.

3. Trends of electron affinity

 this measures the tendency for an atom to gain electron . this is caused by the filling of the valency shell. The trend increases across the period  and decreases down the group  due the electron entering an orbit far away from the nucleus

4. Trend of ionization energy:

Another periodic trend that you will be expected to know is the trend for ionization energy. Ionization energy is defined as the amount of energy required to remove the most loosely bound electron of an atom. How tightly bound the electrons of an atom are will affect the amount of energy required to remove one of the valence electrons. Electrons that are closer to the nucleus are going to be more tightly held than those that are further away and will require more energy to pull them off of the atom. For this reason, we see that ionization energy decreases as you go down a family group and the atoms get larger. This same concept can be applied to atoms across a period. We will see that the highest ionization energy will be found on the right side of the period where the atoms are the smallest, and the lowest ionization energy on the left where the atoms have a larger radii. In general, ionization energy decreases as you go down a family group, and increases as you go across a period from left to right

6. Trend of atomic radius;

One important trend to be aware of is the way that atomic size changes as you move across a period or down a group in the periodic table. Atomic size is typically measured by the radius of the atom starting at the core of the nucleus, and reaching all the way out to the last valence electron.

As you may predict, atomic size will increase as you move down a family group, due to the increased number of electron shells.  This substantially increases the size of the electron cloud. What you may not so easily predict is that atomic size decreases as you go across a period.

Although this may seem counter-intuitive, the decrease in size can be explained by thinking about the valence electron shell as you go across a period; we see that each element across a period has the same valence electron shell that it is filling with valence electrons. While the valence shell stays the same as you go across a period, the number of protons is increasing. Protons, being positively charged, have a pull on the negatively charged electrons out in the electron cloud.

 As the number of protons and electrons increases across a period, they have an attractive pull on one another.  This results in a tightening of the electron cloud and a reduction in the atomic nuclei. In other words, because the outermost electron shell remains the same across a period, that shell gets pulled progressively closer and closer to the nucleus of the atom as you go across a period. So the overall periodic trend for atomic radius (size) is that atoms get smaller as you go across a period, and they get larger as you go down a family group

8.Trends of metallic /nonmetallic properties.

Metallic character refers to the level of reactivity of a metal. Metals tend to lose electrons in chemical reactions, as indicated by their low ionization energies. Within a compound, metal atoms have relatively low attraction for electrons, as indicated by their low electronegativities. By following the trend summary in the figure below, you can see that the most reactive metals would reside in the lower left portion of the periodic table. The most reactive metal is cesium, which is not found in nature as a free element. It reacts explosively with water and will ignite spontaneously in air. Francium is below cesium in the alkali metal group, but is so rare that most of its properties have never been observed.

The metallic character increases as you go down a group. Since the ionization energy decreases going down a group (or increases going up a group), the increased ability for metals lower in a group to lose electrons makes them more reactive. In addition, the atomic radius increases going down a group, placing the outer electrons further away from the nucleus and making that electron less attracted by the nucleus.

Nonmetals tend to gain electrons in chemical reactions and have a high attraction for electrons within a compound. These tendencies are known as nonmetallic character. The most reactive nonmetals reside in the upper right portion of the periodic table. Since the noble gases are a special group because of their lack of reactivity, the element fluorine is the most reactive nonmetal. It is not found in nature as a free element. Fluorine gas reacts explosively with many other elements and compounds and is considered to be one of the most dangerous known substances.

Note that there is no clear division between metallic and nonmetallic character. As we move across the periodic table, there is an increasing tendency to accept electrons (nonmetallic) and a decrease in the possibility that an atom would give up one or more electrons

9. Trends of melting and boiling points:

Melting and boiling points increases from the right of the periodic table until it reaches aluminum and silicon when melting point and boiling point again begin to decrease.

10. Trends in reactivity:

Reactivity refers to how likely or vigorously an atom is to react with other substances

For metals, reactivity decreases from left to right across the period and increases down from top to bottom of the group.

For non-metals, the reactivity increases from left to right across the period and decreases down the group

An illustration showing Summary of Major Periodic Trends

 

 

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